2-METILTIOBENZOKSAZOLNING KOBALT BILAN HOSIL QILGAN KOMPLEKSINI SINTEZI, TUZILISHI VA FIZIK-KIMYOVIY XOSSALARI
##plugins.themes.bootstrap3.article.main##
Annotatsiya
Ushbu ishda kobaltning 2-metiltiobenzoksazol bilan kompleksini sintez qilish, tuzilishi va xossalarini o‘rganishga bag‘ishlangan natijalar keltirilgan. Hosil boʻlgan kompleksning tuzilishi va xossalari rentgen tuzilish tahlil usuli yordamida o‘rganilgan. Kristal monoklinik singoniyaga ega, fazoviy guruhi P21/c (№. 15), a=16.5799 (8), b=9.8956 (4), c=19.1097 (9) Å, β=112.925 (6), V=2887.7 (2) Å3. Kristall tuzilishida kobalt atomiga ikkita ligand molekulasi monodentat holatda, ikkita nitrat ioni bidentat holatda bog‘langan oktaedr tuzlishga ega. Moleklulararo ta’sirlarni vizuallashtirish maqsadida Hirschfeld sirt tahlili o‘tkazilgan.
##plugins.themes.bootstrap3.article.details##
Tsya robota litsenzuetsya vydpovídno do Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 xalqaro litsenziyasi.
Foydalaniladigan adabiyotlar
KiranK. R. et al.(2019). Acid-Catalyzed Condensation of o-Phenylenediammines and o-Aminophenols with α-Oxodithioesters: A Divergent and Regioselective Synthesis of 2-Methylthio-3-aryl/Heteroarylquinoxalines and 2-Acylbenzoxazoles //Synthesis.. – Т. 51. – №. 22. – С. 4205-4214.
Bhat R., Kumbhar P., Helavi V. (2019). Synthesis, characterization and evaluation of antibacterial and antifungal activity of 2-mercaptobenzothiazole and 2-mercaptobenzoxazole derivatives//Chemistry & Biology Interface.V. 9.N.1.P.38-58.
Wang L. et al. (2014) Synthesis of 2-substituted pyrimidines and benzoxazoles via a visible-light-driven organocatalytic aerobic oxidation: enhancement of the reaction rate and selectivity by a base //Green chemistry.Т. 16. №. 8.С. 3752-3757.
Wu F. L. et al. 2-Mercaptobenzothiazole and its derivatives: syntheses, reactions and applications //Current Organic Chemistry. – 2012. – Т. 16. – №. 13. – С. 1555-1580.
Губанова П. А., Рамш С. М. (2010). Особенности спектров 1Н ЯМР четвертичных солей бензазолов в ДМСО-D6//Известия Санкт-Петербургского государственного технологического института (технического университета). №. 7.С. 54-57.
Mohammed O. A., Dahham O. S. (2018). Synthesis, Characterization, and Study of Antibacterial Activity of Some New Formazan Dyes Derivatives, Derived from 2-Mercapto Benzoxazole //IOP Conference Series: Materials Science and Engineering. IOP Publishing, Т. 454. – №. 1. – С. 012-015.
Balogun M. M. et al. (2021). 2‐Mercapto Benzoxazole Derivatives as Novel Leads: Urease Inhibition, In Vitro and In Silico Studies // Chemistry Select. Т. 6. №. 33. С. 8490-8498.
Askar F. W., Hassan H. A., Jinzeel N. A. (2013). Synthesis of Some Heterocyclic Compounds Derived from 2-Mercapto Benzoxazole //Baghdad Science Journal. Т. 10. №. 3.С. 766-778.
Parham H., Khoshnam F. (2013). Solid phase extraction–preconcentration and high performance liquid chromatographic determination of 2-mercapto-(benzothiazole, benzoxazole and benzimidazole) using copper oxide nanoparticles //Talanta. Т. 114. С. 90-94.
Jain C. et al. (2014). Synthesis and Biological activity of organophosphates phenoxy derivatives derived from 2-mercapto benzoxazole //Phosphorus, Sulfur, and Silicon and the Related Elements. Т. 189. №. 11.С. 1699-1705.
Jadhava R. R. et al. (2011). Synthesis of some novel benzoxazole derivatives and their antimicrobial activity //Journal of Pharmacy Research. Т. 4. №. 10. С. 3562-3565.
Spackman, M. A. &Jayatilaka, D. (2009).Hirshfeld surface analysis // Cryst. Eng. Comm. Vol. 11. P. 19-32.
M.Kinnon J.J., Jayatilaka D., Spackman M.A. (2007). Towards quantitative analysis of intermolecular interactions with Hirshfeld surfaces // Chemical Communications. №. 37. P. 3814-3816.
Spackman, P. R., Turner, M. J., McKinnon, J. J., Wolff, S. K., Grimwood, D. J., Jayatilaka, D. & Spackman, M. A. (2021).Crystal Explorer: a program for Hirshfeld surface analysis, visualization and quantitative analysis of molecular crystals // J. Appl. Cryst. Vol. 54. -P. 1006–1011.