2-IZOPROPIL-5-METILFENIL 2-((DIETILKARBAMOTIOYEL) TIO) ASETAT SINTEZI

Normurodov Ilyos O‘rolovich Normurodov Ilyos O‘rolovich; Choriyev Azimjon Uralovich Choriyev Azimjon Uralovich; Xudoyberdiyeva Ozoda Otabek qizi Xudoyberdiyeva Ozoda Otabek qizi; Abdushukurov Anvar Kabirovich Abdushukurov Anvar Kabirovich

Chemistry

No. 1 (2024): FarDU.Ilmiy xabarlar jurnali (Aniq va tabiiy fanlar)

SYNTHESES OF 2-ISOPROPYL-5-METHYLPHENYL 2-((DIETHYLCARBAMOTHIOYL) THIO) ACETATE

Normurodov Ilyos O‘rolovich Normurodov Ilyos O‘rolovich^▸^▾
Choriyev Azimjon Uralovich Choriyev Azimjon Uralovich^▸^▾
Xudoyberdiyeva Ozoda Otabek qizi Xudoyberdiyeva Ozoda Otabek qizi^▸^▾
Abdushukurov Anvar Kabirovich Abdushukurov Anvar Kabirovich^▸^▾

PDF (Uzbek)

Submitted: April 8, 2024
Published: 2024-04-18

Abstract

The article presents the reaction of O-chloroacetylthymol with sodium diethyldithiocarbamate. 2-Isopropyl-5-methylphenyl 2-((diethylcarbamothioyl) thio) acetate was obtained in high yield under the conditions of interphase catalysis. The structures of the obtained compounds were studied by ¹H- and ¹³C- NMR spectroscopy methods.

References

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Li J.J. Name Reactions. A Collection of Detailed Mechanisms and Synthetic Applications. Berlin-Heidelberg, 2009. 704 p.
Reichardt C. Solvents and Solvent Effects in Organic Chemistry, 2nd ed., VCH, NY, 1988. 534 p.
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Гейсс Ф. Основы тонкослойной хроматографии. М.: Мир, 1999. 405 с.
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[1] Choriyev A.U., Abdushukurov A.K., Jurayev R.S., Qaxxorov N.T. O-xloratsetiltimol asosida optik faol birikmalar sintez qilish. FarDU. ILMIY XABARLAR, 2023, no. 1, pp. 76-80.

[2] Dehmlow, E. V., and S. S. Dehmlow, Phase Transfer Catalysis, 3rd ed., Verlag Chemie, Weinheim (1993).

[3] Вебер В., Гокель К. Межфазный катализ в органическом синтезе. Пер. с англ.-М.: Мир,1980.

[4] Li J.J. Name Reactions. A Collection of Detailed Mechanisms and Synthetic Applications. Berlin-Heidelberg, 2009. 704 p.

[5] Reichardt C. Solvents and Solvent Effects in Organic Chemistry, 2nd ed., VCH, NY, 1988. 534 p.

[6] M. Makosza and M. Fedorynski. In Handbook of Phase Transfer Catalysis, Y. Sasson, R. Neumann (Eds.), Chapman & Hall, London (1995).

[7] Гейсс Ф. Основы тонкослойной хроматографии. М.: Мир, 1999. 405 с.

[8] R.M. Silverstein, G. C Bassler and T. C. Morrill, 1998 Spectometric Identification of Organic Compounds (6th Edn) (John Wiley) N.Y.