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O‘zbekcha

SYNTHESES OF 2-ISOPROPYL-5-METHYLPHENYL 2-((DIETHYLCARBAMOTHIOYL) THIO) ACETATE

Authors

  • Toshkent kimyo- texnologiya instituti Shaxrisabz filiali
  • Qarshi davlat universiteti dotsenti
  • Qarshi davlat universiteti
  • Mirzo Ulug‘bek nomidagi O‘zbekiston Milliy universiteti

Keywords:

Interphase catalysis, O-chloroacetylthymol, sodium diethyldithiocarbamate, nucleophilic substitution, 2-isopropyl-5-methylphenyl 2-((diethylcarbamothioyl)thio)acetate.

Abstract

The article presents the reaction of O-chloroacetylthymol with sodium diethyldithiocarbamate. 2-Isopropyl-5-methylphenyl 2-((diethylcarbamothioyl) thio) acetate was obtained in high yield under the conditions of interphase catalysis. The structures of the obtained compounds were studied by 1H- and 13C- NMR spectroscopy methods.

Author Biographies

  • , Toshkent kimyo- texnologiya instituti Shaxrisabz filiali

    Toshkent kimyo- texnologiya instituti Shaxrisabz filiali o‘qituvchisi

  • , Qarshi davlat universiteti dotsenti

    Qarshi davlat universiteti dotsenti, k.f.f.d. (PhD)

  • , Qarshi davlat universiteti

    Qarshi davlat universiteti magistranti

  • , Mirzo Ulug‘bek nomidagi O‘zbekiston Milliy universiteti

    Mirzo Ulug‘bek nomidagi O‘zbekiston Milliy universiteti professori, k.f.d.,

References

Choriyev A.U., Abdushukurov A.K., Jurayev R.S., Qaxxorov N.T. O-xloratsetiltimol asosida optik faol birikmalar sintez qilish. FarDU. ILMIY XABARLAR, 2023, no. 1, pp. 76-80.

Dehmlow, E. V., and S. S. Dehmlow, Phase Transfer Catalysis, 3rd ed., Verlag Chemie, Weinheim (1993).

Вебер В., Гокель К. Межфазный катализ в органическом синтезе. Пер. с англ.-М.: Мир,1980.

Li J.J. Name Reactions. A Collection of Detailed Mechanisms and Synthetic Applications. Berlin-Heidelberg, 2009. 704 p.

Reichardt C. Solvents and Solvent Effects in Organic Chemistry, 2nd ed., VCH, NY, 1988. 534 p.

M. Makosza and M. Fedorynski. In Handbook of Phase Transfer Catalysis, Y. Sasson, R. Neumann (Eds.), Chapman & Hall, London (1995).

Гейсс Ф. Основы тонкослойной хроматографии. М.: Мир, 1999. 405 с.

R.M. Silverstein, G. C Bassler and T. C. Morrill, 1998 Spectometric Identification of Organic Compounds (6th Edn) (John Wiley) N.Y.

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Published

2024-04-18